Difference between revisions of "Tube Furnace (Tystar 8300)"

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= About =
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==About==
 
The three stack Tystar 8” furnace is used primarily for 3 processes. The processes are dedicated for specific tubes as follows:
 
The three stack Tystar 8” furnace is used primarily for 3 processes. The processes are dedicated for specific tubes as follows:
* '''Tube #1''': SOG curing & low-temp oxidation
 
* '''Tubes #2 and #3''': Dry or wet oxidation of silicon (unprocessed, clean)
 
* '''Tube #3''': General furnace annealing & oxidation, including processed material
 
   
 
*'''Tube #1''': SOG curing & low-temp oxidation
Each process tube can accomodate up to one hundred 8” wafers per cycle. We have boats for 2", 3", 4", 6", 8" and irregular shaped pieces. The maximum temperature is 1050°C for the system. Gases used are O<sub>2</sub>, Steam from DI-H<sub>2</sub>O, N<sub>2</sub>.
 
 
*'''Tubes #2 and #3''': Dry or wet oxidation of silicon (unprocessed, clean)
 
*'''Tube #3''': General furnace annealing & oxidation, including processed material
   
 
Each process tube can accomodate up to one hundred 8” wafers per cycle. We have boats for 2", 3", 4", 6", 8" and irregular shaped pieces. The maximum temperature is 1100°C for the system. Gases used are O<sub>2</sub>, Steam from DI-H<sub>2</sub>O, N<sub>2</sub>.
=Process Information=
 
  +
 
==Process Information==
   
 
Recipe Characterization Data, such as thermal oxidation times, can be found on the recipe page:
 
Recipe Characterization Data, such as thermal oxidation times, can be found on the recipe page:
  +
* [[Thermal Processing Recipes|Thermal Processing Recipes: Tystar 8300]]
+
*[[Thermal Processing Recipes|Thermal Processing Recipes: Tystar 8300]]
  +
 
Use the [http://cleanroom.byu.edu/OxideTimeCalc BYU] or [http://www.lelandstanfordjunior.com/thermaloxide.html Stanford Leland Jr.] Thermal Oxidation Calculators to determine the time and temperature that will be necessary for your process needs. You can "calibrate" your oxidations to the Stanford calculator by adjusting the ''Partial Pressure'' on the calculator to match your experimental data.
 
Use the [http://cleanroom.byu.edu/OxideTimeCalc BYU] or [http://www.lelandstanfordjunior.com/thermaloxide.html Stanford Leland Jr.] Thermal Oxidation Calculators to determine the time and temperature that will be necessary for your process needs. You can "calibrate" your oxidations to the Stanford calculator by adjusting the ''Partial Pressure'' on the calculator to match your experimental data.
   
 
Keep in mind that all process must be 30 minutes in length at a minimum. Processes less than 30 minutes will suffer from poor uniformity because the process tube will not have sufficient time to saturate with O<sub>2</sub> or DI-H<sub>2</sub>O.
 
Keep in mind that all process must be 30 minutes in length at a minimum. Processes less than 30 minutes will suffer from poor uniformity because the process tube will not have sufficient time to saturate with O<sub>2</sub> or DI-H<sub>2</sub>O.
   
  +
===Gases Available===
=Recipes=
 
  +
  +
*N2 (15/5 slpm)
  +
*O2 High-range "O2HI" - 15 slpm
  +
*O2 Low-range "O2LO" - 1 slpm
  +
*All gasses flow through the H2O bubbler, which can optionally be filled with heated water to flow steam, or evacuated (no steam, gas only).
  +
 
==Recipes==
   
 
The following are the available recipes on each furnace tube:
 
The following are the available recipes on each furnace tube:
   
 
'''Tube 1:'''
 
'''Tube 1:'''
  +
* SOG425.001 - ''Spin-On Glass Cure''
 
* ALGAAS.001 - ''Oxidation of AlGaAs''
+
*SOG425.001 - ''Spin-On Glass Cure''
  +
*ALGAAS.001 - ''Oxidation of AlGaAs''
  +
 
'''Tube 2:'''
 
'''Tube 2:'''
  +
* WET1050.002 - ''WetOx at 1050°C''
 
* DRY1050.002 - ''DryOx at 1050°C''
+
*WET1050.002 - ''WetOx at 1050°C''
* WETVAR.002 - ''WetOx, variable temp.''
+
*DRY1050.002 - ''DryOx at 1050°C''
* DRYVAR.002 - ''DryOx, variable temp.''
+
*WETVAR.002 - ''WetOx, variable temp.''
 
*DRYVAR.002 - ''DryOx, variable temp.''
  +
 
'''Tube 3:'''
 
'''Tube 3:'''
* WET1050.003 - ''WetOx at 1050°C''
 
* DRY1050.003 - ''DryOx at 1050°C''
 
* WETVAR.003 - ''WetOx, variable temp.''
 
* DRYVAR.003 - ''DryOx, variable temp.''
 
* ANNEAL.003 - ''Anneal with variable time and temperature''
 
   
 
*WET1050.003 - ''WetOx at 1050°C''
=Useful Information=
 
 
*DRY1050.003 - ''DryOx at 1050°C''
[[Media:TystarMechDrawWaferBoat.pdf|Tystar Wafer Boat Drawing - 4" Wafer with 0.5mm Slots]]
 
 
*WETVAR.003 - ''WetOx, variable temp.''
 
*DRYVAR.003 - ''DryOx, variable temp.''
 
*ANNEAL.003 - ''Anneal with variable time and temperature''
  +
  +
=== Process Limits ===
  +
  +
* '''DRY1050''' may not be run for more than 3hrs. O2 flow is 3SLPM, which is too high to run for more than 3hr.
  +
** Contact supervisor for other options, such as '''''DRYVAR''''' @ 1100°C, or with lower O2 flow.
  +
* '''WET1050''' may not be run for more than 24hrs without authorization. Contact supervisor if need to run longer.
  +
* No recipe should be run with >1slpm gas flow without discussing with supervisor first, or gas bottles will be depleted very fast and likely run out during your process.
  +
  +
===[[Thermal Processing Recipes#Tystar 8300|<u>Oxidation Rates & Data</u>]]===
  +
''See the above recipes page for data on oxidation rates for standard oxidation recipes.''
  +
 
==Useful Information==
 
[//wiki.nanotech.ucsb.edu/w/images/8/89/TystarMechDrawWaferBoat.pdf Tystar Wafer Boat Drawing - 4" Wafer with 0.5mm Slots]
  +
 
==See Also==
   
=See Also=
 
 
*[http://www.tystar.com/ Tystar] - Manufacturer of the tool
 
*[http://www.tystar.com/ Tystar] - Manufacturer of the tool
 
*[http://cleanroom.byu.edu/OxideThickCalc Silicon Thermal Oxide Thickness Calculator (BYU)] - Use this on-line calculator to calculate times for silicon oxidation.
 
*[http://cleanroom.byu.edu/OxideThickCalc Silicon Thermal Oxide Thickness Calculator (BYU)] - Use this on-line calculator to calculate times for silicon oxidation.
 
*[http://www.lelandstanfordjunior.com/thermaloxide.html Advanced Silicon Thermal Oxide Thickness Calculator (Stanford Leland Jr.)] - Another thermal oxide calculator, with flexibility to vary ''partial pressure'' parameter to calibrate to your own process.
 
*[http://www.lelandstanfordjunior.com/thermaloxide.html Advanced Silicon Thermal Oxide Thickness Calculator (Stanford Leland Jr.)] - Another thermal oxide calculator, with flexibility to vary ''partial pressure'' parameter to calibrate to your own process.
   
=Operational Instructions=
+
==Operational Instructions==
   
*[[media:Tystar Operational Procedure.pdf|Operating Instructions]]
+
*[//wiki.nanotech.ucsb.edu/w/images/8/8a/Tystar_Operational_Procedure.pdf Operating Instructions]

Latest revision as of 11:15, 7 March 2024

Tube Furnace (Tystar 8300)
Tystar.jpg
Tool Type Thermal Processing
Location Bay 4
Supervisor Tony Bosch
Supervisor Phone (805) 893-3486
Supervisor E-Mail bosch@ece.ucsb.edu
Description Tystar 8" 3-Tube Oxidation/Annealing System
Manufacturer Tystar Corporation
Model Tystar 8300
Sign up for this tool


About

The three stack Tystar 8” furnace is used primarily for 3 processes. The processes are dedicated for specific tubes as follows:

  • Tube #1: SOG curing & low-temp oxidation
  • Tubes #2 and #3: Dry or wet oxidation of silicon (unprocessed, clean)
  • Tube #3: General furnace annealing & oxidation, including processed material

Each process tube can accomodate up to one hundred 8” wafers per cycle. We have boats for 2", 3", 4", 6", 8" and irregular shaped pieces. The maximum temperature is 1100°C for the system. Gases used are O2, Steam from DI-H2O, N2.

Process Information

Recipe Characterization Data, such as thermal oxidation times, can be found on the recipe page:

Use the BYU or Stanford Leland Jr. Thermal Oxidation Calculators to determine the time and temperature that will be necessary for your process needs. You can "calibrate" your oxidations to the Stanford calculator by adjusting the Partial Pressure on the calculator to match your experimental data.

Keep in mind that all process must be 30 minutes in length at a minimum. Processes less than 30 minutes will suffer from poor uniformity because the process tube will not have sufficient time to saturate with O2 or DI-H2O.

Gases Available

  • N2 (15/5 slpm)
  • O2 High-range "O2HI" - 15 slpm
  • O2 Low-range "O2LO" - 1 slpm
  • All gasses flow through the H2O bubbler, which can optionally be filled with heated water to flow steam, or evacuated (no steam, gas only).

Recipes

The following are the available recipes on each furnace tube:

Tube 1:

  • SOG425.001 - Spin-On Glass Cure
  • ALGAAS.001 - Oxidation of AlGaAs

Tube 2:

  • WET1050.002 - WetOx at 1050°C
  • DRY1050.002 - DryOx at 1050°C
  • WETVAR.002 - WetOx, variable temp.
  • DRYVAR.002 - DryOx, variable temp.

Tube 3:

  • WET1050.003 - WetOx at 1050°C
  • DRY1050.003 - DryOx at 1050°C
  • WETVAR.003 - WetOx, variable temp.
  • DRYVAR.003 - DryOx, variable temp.
  • ANNEAL.003 - Anneal with variable time and temperature

Process Limits

  • DRY1050 may not be run for more than 3hrs. O2 flow is 3SLPM, which is too high to run for more than 3hr.
    • Contact supervisor for other options, such as DRYVAR @ 1100°C, or with lower O2 flow.
  • WET1050 may not be run for more than 24hrs without authorization. Contact supervisor if need to run longer.
  • No recipe should be run with >1slpm gas flow without discussing with supervisor first, or gas bottles will be depleted very fast and likely run out during your process.

Oxidation Rates & Data

See the above recipes page for data on oxidation rates for standard oxidation recipes.

Useful Information

Tystar Wafer Boat Drawing - 4" Wafer with 0.5mm Slots

See Also

Operational Instructions