Difference between revisions of "Test Data of Etching SiO2 with CHF3/CF4-Fluorine ICP Etcher"

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(added comment about NP vs ND meas, deleted extraneous tables of old non-standard measurements)
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'''''This page is under construction - we are in the process of standardizing and collecting process control data for this tool. -- Demis 2022-02-11'''''
 
 
   
 
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|Low selectivity/etch rate
 
|Low selectivity/etch rate
 
|[https://wiki.nanotech.ucsb.edu/w/images/8/82/30D_08192022_FICP_001.jpg <nowiki>[30D]</nowiki>][https://wiki.nanotech.ucsb.edu/w/images/5/56/CS_08192022_FICP_001.jpg <nowiki>[CS]</nowiki>]
 
|[https://wiki.nanotech.ucsb.edu/w/images/8/82/30D_08192022_FICP_001.jpg <nowiki>[30D]</nowiki>][https://wiki.nanotech.ucsb.edu/w/images/5/56/CS_08192022_FICP_001.jpg <nowiki>[CS]</nowiki>]
 
|-
  +
| colspan="7" |'''''Change in operator - SEMs below (by NP) are erroneously measured to the trench, instead of flat plane.'''''
 
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|5/18/22
 
|5/18/22
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|[https://wiki.nanotech.ucsb.edu/w/images/c/c8/SiO2_Fl_02_45D_001.jpg <nowiki>[1]</nowiki>] [https://wiki.nanotech.ucsb.edu/w/images/8/89/SiO2_Fl_02_CS_001.jpg <nowiki>[2]</nowiki>]
 
|[https://wiki.nanotech.ucsb.edu/w/images/c/c8/SiO2_Fl_02_45D_001.jpg <nowiki>[1]</nowiki>] [https://wiki.nanotech.ucsb.edu/w/images/8/89/SiO2_Fl_02_CS_001.jpg <nowiki>[2]</nowiki>]
|}
 
 
 
{| class="wikitable"
 
| colspan="6" |Fluorine ICP: 3.8mT, 50/'''900W''', CHF3/CF4=10/30sccm, time='''210 sec''''
 
|
 
|-
 
|Date
 
|Sample#
 
|Etch Rate (nm/min)
 
|Etch Selectivity (SiO2/PR)
 
|Averaged Sidewall Angle (<sup>o</sup>)
 
|Observations/Notes
 
|SEM Image
 
|-
 
|11/5/2021
 
|SOFL01
 
|136
 
|1.2
 
|
 
|
 
|[https://wiki.nanotech.ucsb.edu/w/images/f/fe/SOFL0103.pdf]
 
|-
 
|02/09/22
 
|NP_SiO2_Fl_01
 
|
 
|
 
|
 
|Etched for 210s, all of PR was etched off
 
|[https://wiki.nanotech.ucsb.edu/w/images/8/80/SiO2_Fl_01_45D_002.jpg <nowiki>[1]</nowiki>]
 
|}
 
 
 
{| class="wikitable"
 
| colspan="7" |Fluorine ICP: 3.8mT, 50/800W, CHF3/CF4=10/30sccm, time=90 sec
 
|-
 
|Date
 
|Sample#
 
|Etch Rate (nm/min)
 
|Etch Selectivity (SiO2/PR)
 
|Averaged Sidewall Angle (<sup>o</sup>)
 
|Notes/Observations
 
|SEM Images
 
|-
 
|1/28/2021
 
|FE2102
 
|309
 
|0.99
 
|
 
|
 
|[https://wiki.nanotech.ucsb.edu/w/images/0/0b/FE210206.pdf]
 
 
|}
 
|}

Revision as of 00:36, 10 December 2022

Fluorine ICP: 3.8mT, 50/900W, CHF3/CF4=10/30sccm, time=90 sec
Date Sample # Etch Rate (nm/min) Etch Selectivity (SiO2/PR) Averaged Sidewalls Angle Observations/Notes SEM Images (45d, cross section)
11/18/22 ND_FL_111822 268 1.01 [30D][CS]
11/07/22 ND_FL_110722 264.7 0.96 [30D] [CS]
10/24/22 ND_FL_102422 266.7 1.22 [30D][CS]
10/14/22 ND_FL_101422 249 0.82 Image drifted very slightly

in SEM. May account for

low selectivity.

[30D] [CS]
10/3/22 ND_FL_100322 228 1.10 Low etch rate. [30D] [CS]
9/12/22 ND_FL_091222 278 1.33 high selectivity, may be

due to new Si wafer

[30D] [CS]
8/26/22 ND_FL_082622 288 0.97 Low selectivity/e. rate [30D] [CS]
8/22/22 ND_FL_082222 252.7 0.93 Lower selectivity/e. rate [40D] [CS]
8/19/22 ND_Fl_081922 260.7 0.99 Low selectivity/etch rate [30D][CS]
Change in operator - SEMs below (by NP) are erroneously measured to the trench, instead of flat plane.
5/18/22 NP_SiO2_Fl_10 308.7 1.19 still lower etch rate [1] [2]
5/10/22 NP_SiO2_Fl_09 307.3 1.15 *etch rate seems lower* [1] [2]
4/26/22 NP_SiO2_Fl_08 344.7 1.4 [1] [2]
4/20/22 NP_SiO2_Fl_07 354.7 1.11 [1] [2]
4/14/22 NP_SiO2_Fl_06 352.7 1.11 [1] [2]
3/29/22 NP_SiO2_Fl_05 334.7 1.07 [1][2]
3/09/22 NP_SiO2_Fl_04 358.9 1.06 [1] [2]
3/02/22 NP_SiO2_Fl_03 347 1.05 [1] [2]
2/23/22 NP_SiO2_Fl_02 362.7 1.02 [1] [2]